Preparation of electrodeposited source for 65Zn

P. Sahoo; S.V. Narasimhan; S.E. Kannan

doi:10.1007/BF02060862

Preparation of electrodeposited source for 65Zn

P. Sahoo, S.V. Narasimhan, S.E. Kannan

Research output: Contribution to journal › Article › peer-review

11 Citations (Scopus)

Abstract

Electrolytes of alkaline zincate, acidified zinc sulphate, zinc-ammonia, zinc-ammonia-EDTA, zinc-EDTA/NaOH have been examined in order to verify their applicability for electrodeposition (ED) of zinc on stainless steel (SS) disc at ppm level. Operating parameters suitable for ED of zinc at 90% deposition (amount of zinc removed from plating solution) on SS disc using a total 1 ppm zinc in a 5 cm3 bath volume were determined. It helped to prepare radioactive source (65Zn) using inactive Zn as carrier. Speciation of zinc in a Zn-oxalate-EDTA-ammonia bath has been computed. Copyright © 1996 Akadémiai Kiadó. All rights reserved.

Original language	English
Pages (from-to)	3-14
Number of pages	12
Journal	Journal of Radioanalytical and Nuclear Chemistry
Volume	204
Issue number	1
DOIs	https://doi.org/10.1007/BF02060862
Publication status	Published - 1996

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title = "Preparation of electrodeposited source for 65Zn",

abstract = "Electrolytes of alkaline zincate, acidified zinc sulphate, zinc-ammonia, zinc-ammonia-EDTA, zinc-EDTA/NaOH have been examined in order to verify their applicability for electrodeposition (ED) of zinc on stainless steel (SS) disc at ppm level. Operating parameters suitable for ED of zinc at 90% deposition (amount of zinc removed from plating solution) on SS disc using a total 1 ppm zinc in a 5 cm3 bath volume were determined. It helped to prepare radioactive source (65Zn) using inactive Zn as carrier. Speciation of zinc in a Zn-oxalate-EDTA-ammonia bath has been computed. Copyright {\textcopyright} 1996 Akad{\'e}miai Kiad{\'o}. All rights reserved.",

author = "P. Sahoo and S.V. Narasimhan and S.E. Kannan",

note = "Cited By :10 Export Date: 19 June 2018",

year = "1996",

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journal = "Journal of Radioanalytical Chemistry",

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T1 - Preparation of electrodeposited source for 65Zn

AU - Sahoo, P.

AU - Narasimhan, S.V.

AU - Kannan, S.E.

N1 - Cited By :10 Export Date: 19 June 2018

PY - 1996

Y1 - 1996

N2 - Electrolytes of alkaline zincate, acidified zinc sulphate, zinc-ammonia, zinc-ammonia-EDTA, zinc-EDTA/NaOH have been examined in order to verify their applicability for electrodeposition (ED) of zinc on stainless steel (SS) disc at ppm level. Operating parameters suitable for ED of zinc at 90% deposition (amount of zinc removed from plating solution) on SS disc using a total 1 ppm zinc in a 5 cm3 bath volume were determined. It helped to prepare radioactive source (65Zn) using inactive Zn as carrier. Speciation of zinc in a Zn-oxalate-EDTA-ammonia bath has been computed. Copyright © 1996 Akadémiai Kiadó. All rights reserved.

AB - Electrolytes of alkaline zincate, acidified zinc sulphate, zinc-ammonia, zinc-ammonia-EDTA, zinc-EDTA/NaOH have been examined in order to verify their applicability for electrodeposition (ED) of zinc on stainless steel (SS) disc at ppm level. Operating parameters suitable for ED of zinc at 90% deposition (amount of zinc removed from plating solution) on SS disc using a total 1 ppm zinc in a 5 cm3 bath volume were determined. It helped to prepare radioactive source (65Zn) using inactive Zn as carrier. Speciation of zinc in a Zn-oxalate-EDTA-ammonia bath has been computed. Copyright © 1996 Akadémiai Kiadó. All rights reserved.

U2 - 10.1007/BF02060862

DO - 10.1007/BF02060862

M3 - Article

VL - 204

SP - 3

EP - 14

JO - Journal of Radioanalytical Chemistry

JF - Journal of Radioanalytical Chemistry

SN - 0022-4081

IS - 1

ER -

Preparation of electrodeposited source for 65Zn

Abstract

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