Preparation and characterization of nanocomposite soy-carbon nanotubes (SPI/CNTs) adhesive from soy protein isolate

Olawumi O. Sadare; Michael O. Daramola; Ayo S. Afolabi

Preparation and characterization of nanocomposite soy-carbon nanotubes (SPI/CNTs) adhesive from soy protein isolate

Olawumi O. Sadare, Michael O. Daramola, Ayo S. Afolabi

Chemical, Materials & Metallurgical Engineering

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Abstract

The multifunctional properties of carbon nanotubes (CNTs) as nanofiller in polymer matrix have necessitated the development of adhesives with improved bond strength, and water resistance. However, good dispersion and interfacial interaction between adhesive matrix and carbon nanofiller is essential to obtaining the aforementioned properties. An environmentally friendly adhesive to replace formaldehyde and petrochemical adhesive was prepared from soy protein isolate (SPI) by incorporating CNTs as reinforcement. Sonication with mechanical (shear) stirring was a simple and effective approach to obtain the adhesives with rather uniformly dispersed CNTs in the SPI matrix. Characterization technique employed was scanning electron microscopy which showed the homogeneous dispersion of CNTs in SPI using two mixing methods (shear mixing and sonication/mixing). In addition, Fourier transmission infrared (FTIR) spectroscopy was used to analyze the surface functionalities and the type of functional group on the surface of the adhesive nanocomposite. Thermogravimetry analysis (TGA), gave the percentage weight loss and thermal stability of the samples. The result showed that sonication with 30 minutes of mixing gave a homogenous dispersion more than in shear mixing only.

Original language	English
Title of host publication	WCE 2015 - World Congress on Engineering 2015
Editors	S. I. Ao, Len Gelman, Len Gelman, David W.L. Hukins, Andrew Hunter, Alexander M. Korsunsky, S. I. Ao, S. I. Ao
Publisher	Newswood Limited
Pages	1066-1070
Number of pages	5
Volume	2218
ISBN (Electronic)	9789881404701
Publication status	Published - Jan 1 2015
Event	2015 World Congress on Engineering, WCE 2015 - London, United Kingdom Duration: Jul 1 2015 → Jul 3 2015

Other

Other	2015 World Congress on Engineering, WCE 2015
Country	United Kingdom
City	London
Period	7/1/15 → 7/3/15

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All Science Journal Classification (ASJC) codes

Computer Science (miscellaneous)

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Sadare, O. O., Daramola, M. O., & Afolabi, A. S. (2015). Preparation and characterization of nanocomposite soy-carbon nanotubes (SPI/CNTs) adhesive from soy protein isolate. In S. I. Ao, L. Gelman, L. Gelman, D. W. L. Hukins, A. Hunter, A. M. Korsunsky, S. I. Ao, & S. I. Ao (Eds.), WCE 2015 - World Congress on Engineering 2015 (Vol. 2218, pp. 1066-1070). Newswood Limited.

Sadare, Olawumi O. ; Daramola, Michael O. ; Afolabi, Ayo S. / Preparation and characterization of nanocomposite soy-carbon nanotubes (SPI/CNTs) adhesive from soy protein isolate. WCE 2015 - World Congress on Engineering 2015. editor / S. I. Ao ; Len Gelman ; Len Gelman ; David W.L. Hukins ; Andrew Hunter ; Alexander M. Korsunsky ; S. I. Ao ; S. I. Ao. Vol. 2218 Newswood Limited, 2015. pp. 1066-1070

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title = "Preparation and characterization of nanocomposite soy-carbon nanotubes (SPI/CNTs) adhesive from soy protein isolate",

abstract = "The multifunctional properties of carbon nanotubes (CNTs) as nanofiller in polymer matrix have necessitated the development of adhesives with improved bond strength, and water resistance. However, good dispersion and interfacial interaction between adhesive matrix and carbon nanofiller is essential to obtaining the aforementioned properties. An environmentally friendly adhesive to replace formaldehyde and petrochemical adhesive was prepared from soy protein isolate (SPI) by incorporating CNTs as reinforcement. Sonication with mechanical (shear) stirring was a simple and effective approach to obtain the adhesives with rather uniformly dispersed CNTs in the SPI matrix. Characterization technique employed was scanning electron microscopy which showed the homogeneous dispersion of CNTs in SPI using two mixing methods (shear mixing and sonication/mixing). In addition, Fourier transmission infrared (FTIR) spectroscopy was used to analyze the surface functionalities and the type of functional group on the surface of the adhesive nanocomposite. Thermogravimetry analysis (TGA), gave the percentage weight loss and thermal stability of the samples. The result showed that sonication with 30 minutes of mixing gave a homogenous dispersion more than in shear mixing only.",

author = "Sadare, {Olawumi O.} and Daramola, {Michael O.} and Afolabi, {Ayo S.}",

year = "2015",

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Sadare, OO, Daramola, MO & Afolabi, AS 2015, Preparation and characterization of nanocomposite soy-carbon nanotubes (SPI/CNTs) adhesive from soy protein isolate. in SI Ao, L Gelman, L Gelman, DWL Hukins, A Hunter, AM Korsunsky, SI Ao & SI Ao (eds), WCE 2015 - World Congress on Engineering 2015. vol. 2218, Newswood Limited, pp. 1066-1070, 2015 World Congress on Engineering, WCE 2015, London, United Kingdom, 7/1/15.

Preparation and characterization of nanocomposite soy-carbon nanotubes (SPI/CNTs) adhesive from soy protein isolate. / Sadare, Olawumi O.; Daramola, Michael O.; Afolabi, Ayo S.

WCE 2015 - World Congress on Engineering 2015. ed. / S. I. Ao; Len Gelman; Len Gelman; David W.L. Hukins; Andrew Hunter; Alexander M. Korsunsky; S. I. Ao; S. I. Ao. Vol. 2218 Newswood Limited, 2015. p. 1066-1070.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

TY - GEN

T1 - Preparation and characterization of nanocomposite soy-carbon nanotubes (SPI/CNTs) adhesive from soy protein isolate

AU - Sadare, Olawumi O.

AU - Daramola, Michael O.

AU - Afolabi, Ayo S.

PY - 2015/1/1

Y1 - 2015/1/1

N2 - The multifunctional properties of carbon nanotubes (CNTs) as nanofiller in polymer matrix have necessitated the development of adhesives with improved bond strength, and water resistance. However, good dispersion and interfacial interaction between adhesive matrix and carbon nanofiller is essential to obtaining the aforementioned properties. An environmentally friendly adhesive to replace formaldehyde and petrochemical adhesive was prepared from soy protein isolate (SPI) by incorporating CNTs as reinforcement. Sonication with mechanical (shear) stirring was a simple and effective approach to obtain the adhesives with rather uniformly dispersed CNTs in the SPI matrix. Characterization technique employed was scanning electron microscopy which showed the homogeneous dispersion of CNTs in SPI using two mixing methods (shear mixing and sonication/mixing). In addition, Fourier transmission infrared (FTIR) spectroscopy was used to analyze the surface functionalities and the type of functional group on the surface of the adhesive nanocomposite. Thermogravimetry analysis (TGA), gave the percentage weight loss and thermal stability of the samples. The result showed that sonication with 30 minutes of mixing gave a homogenous dispersion more than in shear mixing only.

AB - The multifunctional properties of carbon nanotubes (CNTs) as nanofiller in polymer matrix have necessitated the development of adhesives with improved bond strength, and water resistance. However, good dispersion and interfacial interaction between adhesive matrix and carbon nanofiller is essential to obtaining the aforementioned properties. An environmentally friendly adhesive to replace formaldehyde and petrochemical adhesive was prepared from soy protein isolate (SPI) by incorporating CNTs as reinforcement. Sonication with mechanical (shear) stirring was a simple and effective approach to obtain the adhesives with rather uniformly dispersed CNTs in the SPI matrix. Characterization technique employed was scanning electron microscopy which showed the homogeneous dispersion of CNTs in SPI using two mixing methods (shear mixing and sonication/mixing). In addition, Fourier transmission infrared (FTIR) spectroscopy was used to analyze the surface functionalities and the type of functional group on the surface of the adhesive nanocomposite. Thermogravimetry analysis (TGA), gave the percentage weight loss and thermal stability of the samples. The result showed that sonication with 30 minutes of mixing gave a homogenous dispersion more than in shear mixing only.

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M3 - Conference contribution

AN - SCOPUS:84991226892

VL - 2218

SP - 1066

EP - 1070

BT - WCE 2015 - World Congress on Engineering 2015

A2 - Ao, S. I.

A2 - Gelman, Len

A2 - Hukins, David W.L.

A2 - Hunter, Andrew

A2 - Korsunsky, Alexander M.

A2 - Ao, S. I.

PB - Newswood Limited

T2 - 2015 World Congress on Engineering, WCE 2015

Y2 - 1 July 2015 through 3 July 2015

ER -

Preparation and characterization of nanocomposite soy-carbon nanotubes (SPI/CNTs) adhesive from soy protein isolate

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